硫二甘醇及其相关氧化产物的硅烷化衍生反应条件优化及应用 |
| |
引用本文: | 吴晓飞,周世坤,刘景全.硫二甘醇及其相关氧化产物的硅烷化衍生反应条件优化及应用[J].防化研究,2007(1):20-23. |
| |
作者姓名: | 吴晓飞 周世坤 刘景全 |
| |
摘 要: | 研究了衍生气相色谱法测定芥子气的降解产物硫二甘醇、硫二甘醇亚砜和硫二甘醇砜的方法,并对影响衍生反应的溶剂、温度、时间和衍生试剂用量进行了优化,该法操作简便、灵敏度高。
|
关 键 词: | 硅烷化衍生方法 硫二甘醇 硫二甘醇亚砜 硫二甘醇砜 气相色谱 |
修稿时间: | 2006-01-08 |
Application and optimization of silylation reaction for the determination of thiodiglycol and oxidation products |
| |
Authors: | Wu Xiaofei Zhou Shikun Liu Jingquan |
| |
Abstract: | A method for determination of thiodiglycol, thiodiglycol sulphoxide and thiodiglycol sulphone by gas chromatography after silylated derivatives are studied. The detection conditions are optimized. The method is convenient and sensitive. |
| |
Keywords: | silylation thiodiglycol thiodiglycol sulphoxide thiodiglycol sulphone GC |
本文献已被 维普 等数据库收录! |