| 5－乙酰基－2－氨基二苯甲酮的合成 |
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| 引用本文： | 张学骜,龙永福,许静,谢凯,安立华.5－乙酰基－2－氨基二苯甲酮的合成[J].国防科技大学学报,2003,25(5):31-35. |
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| 作者姓名： | 张学骜 龙永福 许静 谢凯 安立华 |
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| 作者单位： | 国防科技大学航天与材料工程学院,湖南,长沙,410073 |
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| 基金项目： | 国家部委基金资助项目(51307) |
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| 摘 要： | 用对硝基苯乙酮、乙二醇、苯乙腈、氢气、高氯酸为原料,经酮基保护,环化,催化加氢和消除反应,合成出较高产率的5-乙酰基-2-氨基二苯甲酮。对反应机理作了初步探讨,并用元素分析、IR和1HNMR对其结构进行了表征。
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| 关 键 词： | 5-乙酰基-2-氨基二苯甲酮 合成 表征 |
| 文章编号： | 1001-2486(2003)05-0031-05 |
| 收稿时间： | 2003/3/18 0:00:00 |
| 修稿时间： | 2003年3月18日 |
Synthesis of 5-Acetyl-2-aminobenzophenone |
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| ZHANG XueAo,LONG YongFu,XU Jing,XIE Kai and AN LiHua.Synthesis of 5-Acetyl-2-aminobenzophenone[J].Journal of National University of Defense Technology,2003,25(5):31-35. |
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| Authors: | ZHANG XueAo LONG YongFu XU Jing XIE Kai and AN LiHua |
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| Institution: | College of Aerospace and Materials Engineering, National Univ. of Defense Technology, Changsha 410073, China;College of Aerospace and Materials Engineering, National Univ. of Defense Technology, Changsha 410073, China;College of Aerospace and Materials Engineering, National Univ. of Defense Technology, Changsha 410073, China;College of Aerospace and Materials Engineering, National Univ. of Defense Technology, Changsha 410073, China;College of Aerospace and Materials Engineering, National Univ. of Defense Technology, Changsha 410073, China |
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| Abstract: | The 5-acetyl-2-aminobenzophenone with high yield was synthesized by using p-nitroacetophenone, ethylene glycol, phenylacetonitrile, hydrogen, perchloric acid as raw materials. The reaction mechanism is discussed simply, and the structure of compound is identified by elemental analysis, IR and 1HNMR. |
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| Keywords: | 5-acetyl-2-aminobenzophenone synthesis characteristic |
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