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用1,4-二氯甲基-2,5-二甲基苯和1,4-二氯甲基-2-甲氧基-5-辛氧基苯共聚合成了一种可溶的聚对苯乙炔的衍生物,对共聚物结构进行了红外光谱、核磁共振氢谱表征  相似文献   

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用对硝基苯乙酮、乙二醇、苯乙腈、氢气、高氯酸为原料,经酮基保护,环化,催化加氢和消除反应,合成出较高产率的5-乙酰基-2-氨基二苯甲酮。对反应机理作了初步探讨,并用元素分析、IR和1HNMR对其结构进行了表征。  相似文献   

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用Ⅰ(n=2,4,7,8)的氯甲基化反应合成出相应的四种氯甲基化产物Ⅱ(n=2,4,7,8),讨论了反应条件对产率的影响,产物结构由IR和1HNMR确定,并讨论了反应机理。CH3OO(CH2)nH(Ⅰ)CH3OCH2C1O(CH2)nHCH2C1(Ⅱ  相似文献   

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Africa has emerged as a strategic location for transcontinental narcotics trade. Particularly the West African subcontinent has turned into a cocaine warehousing and trans-shipment hub along the way to the European underground markets. At this juncture, African drug networks (ADNs) began to play a momentous role in global drug trade, and pose a considerable threat to international security, as they operate in more than 80 countries. The United Nations Office on Drugs and Crime, Interpol, and Europol perceive ADNs as one of the primary issues in international counter-narcotics policy. These agencies have launched several multilateral initiatives to contain the West African threat. None of these initiatives, however, retarded the expansion of the problem. Indeed, the containment efforts turned out to be quite embryonic. The ADNs eventually entered the Turkish market by the early 2000s. West African drug networks (WADNs) in particular have begun to operate within Turkey extensively, often supplying and distributing drugs. The gravity of the threat became ever more serious by 2012. The upsurge of the new threat has compelled the Turkish drug-law enforcement agencies to adopt new policies and counter-strategies. These policies have to be based upon proper strategic analysis of the threat. This paper seeks to address the need for a threat assessment of ADNs. It investigates the dimensions of the problem, profiles the members of WADNs, their modes of operation, and the factors that compelled them to exploit the illicit Turkish drug markets. The analyses are based upon the scrutiny of 227 narcotic interdictions files and statements from the African individuals in these case files. The paper concludes by presenting policy implications and recommendations for the Turkish security and foreign-policy institutions to cope with this impending threat.  相似文献   

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本文用对甲氧基苯酚、正溴丁烷、聚甲醛为原料, 经醚化, 双氯甲基化和碱性消除反应, 合成出长链共轭且可溶的聚(2甲氧基5丁氧基)亚苯基亚乙烯,用 I R 和1 H N M R 表征了中间体和聚合物的结构,并测定了聚合物的伏—安特性曲线。  相似文献   

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本文总结了郑和号训练舰主动力推进装置舰员级维修需求卡PCSM的研制过程和经验,阐述了PCSM的组成和使用方法,对提高我军舰船维修理论水平和维修实践具有重要指导意义。  相似文献   

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围绕J=1/2,2水平椭圆柱的有限长接触熔化   总被引:1,自引:0,他引:1  
研究相变材料围绕J =1/2 ,2水平椭圆柱在有限长接触时的温差熔化过程 .应用边界层理论求得熔化边界层厚度 ,作用力与熔化速度关系式 .讨论了有关结果 ,并与长椭圆柱以及有限长圆柱的温差熔化的结果进行了比较 ,给出一些有益的结论  相似文献   

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本文介绍了采用微处理机技术的JD-5W型电磁计程仪的基本工作原理、硬件组成及程序设计。该仪器不但结构简单、解算与传送精度高、接口功能齐全,而且在测速校正过程中能自动完成数据处理与误差修正,解决了计程仪使用过程中测速校正困难的问题。  相似文献   

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本文研究了最佳(n,2,w)二进制等重检错码的存在性问题。对于文[5]中n 为偶数时所得的结论,本文给了一个简练的证明。更为重要的是,利用以上方法,作者证明了文[5]中关于n 为奇数时的一个猜想。  相似文献   

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介绍了双环原酸酯个4-羟甲基-2,6,7-二氧杂二环(2.2.2)辛烷的合成方法,并提供了一条简单可行的合成途径.  相似文献   

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The component placement problem is a specialization of the quadratic assignment problem that has been extensively studied for a decade and which is of considerable practical value. Recently, interest in component placement algorithms has risen primarily as a result of increased activity in the field of computer-aided design automation. This paper deals with the methodology of component placement and is based on the results of considerable operational experience. A tutorial presentation of tree search placement algorithms is provided, and an improved placement procedure is described which is demonstrated to be effective in generating near optimal solutions to the component placement problem. These solutions are completely reproducible and are obtained at an acceptable expenditure of computational resources. An additional objective is an assessment of performance of the class of near optimal algorithms. In particular, the question- how close to optimal are the near optimal solutions- is examined.  相似文献   

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