羰基化合物亚甲基化方法的研究

Takai试剂（CH2I2-Zn-TiCl4）作为亚甲基化试剂能高效地使羰基亚甲基化,这一方法与运用Wittig试剂等方法相比,反应条件更加温和、副产物更少、合成成本较低且收率高。     

小学课堂师生互动研究---基于课堂视频分析方法的探讨

学生和教师相互交流、共同发展的过程是学校教育情境中师生互动的最基本的形式.注重师生之间的关系,构建有效的师生互动方式,能够促进学生和教师的共同成长.研究以石河子市Y小学作为研究对象,采用访谈和视频录像分析相结合的方法,分析小学课堂师生互动的成效.从研究收集到的18节语文、数学课录像发现:教师提问与学生回答频次相当;数学课教师提问频次多于语文课教师;学生回答问题的积极性高;新手教师以讲述为主,专家型教师多进行课堂互动;小学课堂互动以师个互动为主,并且随年级的升高呈现递减趋势.由此提出增强教师的研究意识、改善教学环境、评价方式多样化等提高课堂师生互动有效性的建议,为小学课堂师生互动的理论研究与实践提供参考.     

The investigation of NTO/HMX-based plastic-bonded explosives and its safety performance

3-nitro-1,2,4-triazol-5-one (NTO) is the main component of insensitive munitions (IM) formulation because of its outstanding insensitive properties.In this paper,a series of NTO/HMX-based composite explosives were prepared and characterized.The study focuses on the effect of NTO on the performance of the formulations,especially the safety performance.The results revealed that the mechanical sensi-tivity of formulations was associated with NTO content,as well as the thermal conductivity,specific heat capacity and Arrhenius parameters.Then,the high amount of NTO using in formulation was proved to be helpful for NTO/HMX-based formulation to exhibit good thermal safety.Besides,by accelerating rate calorimeter (ARC) and a modified cook-offequipment,the pressure and pressure rise rate were proved as the important indicator for judging the thermal safety performance in confined spaces.Finally,the numerical simulation was used as a credible method for predicting the respond temperature of cook-off experiment.     

某型导弹并联挂架维修性试验方法研究

结合维修性试验的一般要求和方法,充分考虑新研设备维修性试验中遇到的具体问题,提出了某型导弹并联挂架维修性试验方法。     

Hazard evaluation of ignition sensitivity and explosion severity for three typical MH2 (M＝Mg,Ti, Zr) of energetic materials

MgH2, TiH2, and ZrH2 are three typical metal hydrides that have been gradually applied to composite explosives and propellants as additives in recent years. To evaluate ignition sensitivity and explosion severity, the Hartmann device and spherical pressure vessel were used to test ignition energy and ex-plosion pressure, respectively. The results showed that the ignition sensitivity of ZrH2, TiH2 and MgH2 gradually increased. When the concentration of MgH2 is 83.0 g/m3 in Hartmann device, the ignition energy attained a minimum of 10.0 mJ. The explosion pressure of MgH2 were 1.44 times and 1.76 times that of TiH2 and ZrH2, respectively, and the explosion pressure rising rate were 3.97 times and 9.96 times that of TiH2 and ZrH2, respectively, through the spherical pressure vessel. It indicated that the reaction reactivity and reaction rate of MgH2 were higher than that of TiH2 and ZrH2. In addition, to conduct in-depth theoretical analysis of ignition sensitivity and explosion severity, gas production and combus-tion heat per unit mass of ZrH2, TiH2 and MgH2 were tested by mercury manometer and oxygen bomb calorimetry. The experimental results revealed that MgH2 had a relatively high gas production per unit mass (5.15 mL/g), while TiH2 and ZrH2 both had a gas production of less than 2.0 mL/g. Their thermal stability gradually increased, leading to a gradual increase in ignition energy. Furthermore, compared with theoretical combustion heat, the combustion ratio of MgH2, TiH2 and ZrH2 was more than 96.0%, with combustion heat value of 29.96, 20.94 and 12.22 MJ/kg, respectively, which was consistent with the explosion pressure and explosion severity test results.     

光栅过滤法测试陶瓷磨削表面残余应力

采用表面形貌技术对陶瓷磨削表面残余应力进行测试研究,对表面粗糙度曲线经过数据截取、滤波以及规范化处理后可得到表面挠度曲线,认为,此方法与X射线衍射法相比测试结果较接近,是测试残余应力的有效方法;其数据处理过程是保证测试精度的关键;挠度变化是个渐变的过程。     

射击与通信实践环节的综合训练

以院实施射击、通信课改革为出发点,针对改革实施的必要性、指导思想、改革的内容、改革的措施等几个问题进行了具体论述。为下一步改革提供几点借鉴,促进改革的顺利实施。     

中频同步发电机组励磁系统的改进

用ＰＷＭ调节技术,按自控原理,对发电机励磁系统进行了改进设计,并比较了几种励磁系统的优缺点,提出了完整的设计电路。其电路简单,工作可靠。     

频率捷变雷达干扰方法分析

频率捷变雷达有许多其它雷达无法比拟的优点,在现代雷达体制中占有重要地位。分析了频率捷变雷达的特点,根据其工作原理,提出了干扰频率捷变雷达的几种方法,分析了各自的优点和局限性。阐述了干扰方法的原理及实现的技术途径,并给出了有关参数的计算方法和实例。     

科学发展观的政治意蕴

马克思主义是人类第一个建立在科学方法论基础上的社会发展理论,科学发展观是马克思主义社会发展理论的继承和发展。注重研究政治功能,在马克思主义社会发展学说中显得十分突出。无论从科学发展观提出的现实背景、过程,还是核心和主题词来看,都有十分突显的政治意蕴。尤其是“以人为本”,既承授了马克思人的自由和解放的命题,又突出以社会主义国家政权的力量来维护社会的平等和公正,科学发展观蕴含和展现的这一政治意蕴,是极为重要的和不可忽略的。