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71.
72.
To explore the effect of different positions and number of pyrrolidine bound to the carbon cage on the stabilization effect of fulleropyrrolidine derivatives to nitrocellulose (NC)/nitroglycerine (NG), we synthesized N-(4-methoxy) phenylpyrrolidine-C60 and four different of bis(N-(4-methoxy) phenylpyrrolidine)-C60 compounds through Prato reaction. Their structures were characterized by UV–vis, 1H NMR, 13C NMR, high-resolution mass spectroscopy, and single-crystal X-ray diffraction. Their stabilization effect to NC/NG were investigated using differential scanning calorimetry, methyl violet, vacuum stabilization effect, weight loss, and accelerating rate calorimeter tests. The results indicated these compounds had excellent stabilization effect to NC/NG. The stabilization effect of the fulleropyrrolidine bisadducts to NC/NG is significantly better than that of fulleropyrrolidine monoadduct and C60. Moreover, the position where pyrrolidine binds to fullerene in fulleropyrrolidine bisadducts is different, and its stabilization effect to NC is also different. The stabilization effect order of different bisadduct isomers to nitrocellulose is as follows: e-edge > trans-2> cis-2> trans-3. Electron paramagnetic resonance (EPR) and FT-IR were used to study the stabilization mechanism of fulleropyrrolidine derivatives to NC/NG. The EPR results also show that fulleropyrrolidine bisadducts with different addition sites have different abilities to absorb nitroxide, and their ability is better than that of the monoadduct and C60, which is consistent with the results of stabilization effect performance test. 相似文献
73.
指挥控制通信与情报(C3I)系统的评价 总被引:5,自引:0,他引:5
综述了目前用于评价C3I系统的各类方法与过程,讨论了C3I系统的评价框架,并对这个框架下的各种评价方法与过程的长处和不足提出了作者的看法 相似文献
74.
基于RTP协议H.264视频流传输QoS保证的研究 总被引:2,自引:0,他引:2
提出一个Linux环境下基于RTP/RTCP的H.264视频流传输的方案,在Linux中调用V4L(VideofourLinux)的API函数采集视频流,经X264压缩,RTP/RTCP协议打包进行传输。并通过RTCP的RR(接收方报告)包反馈信息和吞吐量公式来计算近似带宽,以起始帧量化参数start-qp为视频编码的调节参数,由近似带宽来控制视频编码的参数调整,达到控制输出码率的目的,实现对视频传输的QoS(QualityofService)保证。 相似文献
75.
美军作战实验室建设研究 总被引:1,自引:0,他引:1
简要回顾了美军作战实验发展的历史,从军种到联合详细阐述了美军作战实验室完整的体系,并简要介绍了各作战实验室所完成的典型实验,研究了美军作战实验室主要的实验方法和技术手段,剖析了美军作战实验室的运行机制,探讨了美军作战实验室建设带给我们的启示。 相似文献
76.
针对径向基(RBF)神经网络在进行超声检测脱粘缺陷识别时存在参数选择不确定、网络结构鲁棒性差等问题,提出一种改进的自适应半监督模糊C均值聚类(FCM)的RBF神经网络的方法,将kw近邻估计法和半监督模糊C均值聚类方法相结合,改进了隶属度函数,自适应确定聚类数目。将改进的RBF神经网络应用于超声检测脱粘缺陷识别,实验结果表明:与传统RBF神经网络相比,本方法减弱了孤立样本对网络结构的影响,增强了网络结构的鲁棒性,提高了脱粘缺陷识别的准确率,是一种较好的超声检测脱粘缺陷识别分类方法. 相似文献
77.
The mechanical, thermal and ablation properties of carbon phenolic (C-Ph) composites (Type-I) rein-forced with different weight percentages of organo-modified montmorillonite (o-MMT) nanoclay have been studied experimentally. Ball milling was used to disperse different weight (wt) percentages (0, 1,2,4,6 wt.%) of nanoclay into phenolic resin. Viscosity changes to resin due to nanoclay was studied. On the other hand, nanoclay added phenolic matrix composites (Type-II) were prepared to study the dispersion of nanoclay in phenolic matrix by small angle X-ray scattering and thermal stability changes to the matrix by thermogravimetric analyser (TGA). This data was used to understand the mechanical, thermal and ablation properties of Type-I composites. Inter laminar shear strength (ILSS), flexural strength and flexural modulus of Type I composites increased by about 29%, 12%and 7%respectively at 2 wt.% addition of nanoclay beyond which these properties decreased. This was attributed to reduced fiber volume fraction (%Vf) of Type-I composites due to nanoclay addition at such high loadings. Mass ablation rate of Type-I composites was evaluated using oxy acetylene torch test at low heat flux (125 W/cm2) and high heat flux levels (500 W/cm2). Mass ablation rates have increased at both flux levels marginally up to 2 wt.% addition of nanoclay beyond which it has increased significantly. This is in contrast to increased thermal stability observed for Type-I and Type-Ⅱ composites up to 2 wt.%addition of nanoclay. Increased ablation rates due to nanoclay addition was attributed to higher insulation effi-ciency of nanolcay, which accumulates more heat energy in limited area behind the ablation front and self-propagating ablation mechanisms triggered by thermal decomposition of organic part of nanoclay. 相似文献
78.
为构建一体化的空天作战信息环境,面向大情报系统的信息共享和应用重组集成目标,探讨了以信息服务理念架构大情报系统的总体思路,总结筛选了大情报系统信息服务组件开发与集成应遵循的技术规范与标准.有助于大情报系统的体系结构设计,高效集成多元化的现有或即将建设的关联系统,并逐步过渡到统一的信息技术体制上. 相似文献
79.
We study a stochastic inventory model of a firm that periodically orders a product from a make‐to‐order manufacturer. Orders can be shipped by a combination of two freight modes that differ in lead‐times and costs, although orders are not allowed to cross. Placing an order as well as each use of each freight mode has a fixed and a quantity proportional cost. The decision of how to allocate units between the two freight modes utilizes information about demand during the completion of manufacturing. We derive the optimal freight mode allocation policy, and show that the optimal policy for placing orders is not an (s,S) policy in general. We provide tight bounds for the optimal policy that can be calculated by solving single period problems. Our analysis enables insights into the structure of the optimal policy specifying the conditions under which it simplifies to an (s,S) policy. We characterize the best (s,S) policy for our model, and through extensive numerical investigation show that its performance is comparable with the optimal policy in most cases. Our numerical study also sheds light on the benefits of the dual freight model over the single freight models. © 2011 Wiley Periodicals, Inc. Naval Research Logistics, 2011 相似文献
80.
造型技术是CAD/CAM的核心技术。本文较详细地介绍了几何造型、壳体造型及特征造型的理论与算法,分析了各种造型方法及形体表示方法的优缺点,最后探讨了造型技术的发展趋势。 相似文献