路易氏剂衍生物的气相色谱-质谱研究

用一种单巯基化合物1-巯基丙烷和三种双巯基化合物1,3-二巯基丙烷、2,3-二巯基丙醇、3,4-二巯基甲苯经亲核取代反应将路易氏剂衍生为挥发性较好的二硫砷化合物,用GC-MS鉴定了这些化合物的结构,并讨论了分子离子的碎裂方式及个别碎片的来源．     

面向对象的燃气发生器地面试验柔性控制模型与实现

根据燃气发生器地面试验对控制的需求,分析了其控制行为,提出了面向对象的燃气发生器地面试验柔性控制模型。模型先进合理,符合目前测控技术发展的方向。在该模型基础上实现了柔性控制系统,能够满足各种型号的燃气发生器地面试验对控制的需求,并在试验中得到了成功的应用。与以前的控制系统相比,该系统具有可靠性高、结构简单、操作简单灵活等特点。     

On the median residual lifetime and its aging properties: A characterization theorem and applications

This paper is devoted to study several aspects of the median residual life function (MERLF). In reliability studies, it is well known that, although the MERLF have several advantages over the mean residual life function (MRLF), the MRLF has the good property of uniquely determine a life distribution whereas either the median residual life function (MERLF) or an α‐percentile residual life do not have such good property. We shall give a characterization result where knowledge of both the MERLF and the survival function on an interval does uniquely determine the distribution. Moreover, in order to apply this characterization in practical situations, we propose a method to estimate the necessary information of the survival function. Relationships between analytical properties of the survival function and its associated MERLF are also obtained. Bryson and Siddiqui [J Am Statist Assoc 64 (1969), 1472–1483] proved relationships among seven criteria for aging, out of which two contained the MRLF (decreasing MRLF and net decreasing MRLF). In this paper, we prove that the same pattern of relationships holds if the MRLF is replaced by the MERLF. We also examine the aging criteria corresponding to an increasing MERLF and show that there is no relation between the behavior (increasing or decreasing) of the MERLF and of the MRLF. © 2005 Wiley Periodicals, Inc. Naval Research Logistics, 2005     

新型涂层固相微萃取-气相色谱分析检测VX

以溶胶凝胶和交联固化相结合的方法制备了杯[4]芳烃开链冠醚／羟基硅油（Calix[4]open chain ether／OH-TSO）复合涂层固相微萃取探头,采用固相微萃取与气相色谱联用的方法测定水和土壤中的VX．并对自制探头的萃取效率、热稳定性、抗溶剂冲洗能力、使用寿命,保质期以及探头制备重现性等性能进行了系统研究．     

长杆射弹对钢纤维混凝土靶开坑特性的实验研究

为考察射弹对钢纤维混凝土靶的侵彻特性,采用57mm轻气炮,进行了小尺寸模拟射弹对钢纤维混凝土靶(钢纤维的体积分数为2%)的侵彻实验。实验中观察了钢纤维混凝土靶的开坑形状,测量了射弹的击靶速度,并且采用注沙法测出靶体的开坑体积,计算出射弹对靶体的侵彻体积,得到了长杆射弹的动能与侵彻体积的关系。引入射弹单位面积的冲击动能和靶体单位侵彻体积的冲击动能,结合钢纤维混凝土靶的实验数据,考察了两者之间的关系。     

Some new results on the preservation of the NBUE and NWUE aging classes under the formation of coherent systems

We consider the classical problem of whether certain classes of lifetime distributions are preserved under the formation of coherent systems. Under the assumption of independent and identically distributed (i.i.d.) component lifetimes, we consider the NBUE (new better than used in expectation) and NWUE (new worse than used in expectation) classes. First, a necessary condition for a coherent system to preserve the NBUE class is given. Sufficient conditions are then obtained for systems satisfying this necessary condition. The sufficient conditions are satisfied for a collection of systems which includes all parallel systems, but the collection is shown to be strictly larger. We also prove that no coherent system preserves the NWUE class. As byproducts of our study, we obtain the following results for the case of i.i.d. component lifetimes: (a) the DFR (decreasing failure rate) class is preserved by no coherent systems other than series systems, and (b) the IMRL (increasing mean residual life) class is not preserved by any coherent systems. Generalizations to the case of dependent component lifetimes are briefly discussed.     

多点喷射空气酒精燃气发生器试验验证

为有效解决现有燃气引射气源存在的诸多缺点,适应一种引射系统大流量、小型化的需要,在综合分析各燃气引射气源方案的基础上,研制了一种以空气、酒精作为推进剂的多点喷射结构的燃气发生器,并开展了多种工况下的试验研究。结果表明:采用的多点喷射方案大大提高了空间利用率,有效满足了引射系统小型化的要求;喷雾性能好,喷雾锥角及粒径优于设计指标要求;点火可靠性高,解决了领域内现有燃气发生器点火可靠性低的缺点;点火迅速,燃烧平稳,可实现较为均匀的出口温度场;燃气发生器工作范围较宽,能在余气系数2.52～4.34范围内稳定燃烧;高效的火焰筒内壁空气冷却方式有效保证了燃气发生器长时间工作运行。     

液化石油气火灾的预防及扑救

在分析液化石油气的组成成份及其理化性质的基础上,针对液化石油气的火灾危险性及火灾特点,提出了防火防爆及火灾扑救措施.     

惰性气体中电爆丝爆炸激励冲击波的理论分析

建立了惰性气体中电爆丝爆炸激励的冲击波模型。对于冲击波马赫数与光辐射强度的关系、惰性气体种类对冲击波强度的影响以及电爆丝根数对冲击波强度的影响,进行了理论计算与分析,所得结论对红外脉冲强光辐射源的研究有重要作用。     

营房室内有害气体污染预测研究

由于营房建筑、装饰材料质量不合格,施工工艺不正确等原因,引起营房室内有害气体污染,严重威胁到住用者的生命健康和部队战斗力。研究营房室内有害气体污染变化发展的规律,对营房室内有害气体污染进行准确的预测,做好预防措施,可以避免营房室内有害气体污染的发生。采用灰色预测方法对营房室内有害气体污染水平进行预测,在 GM(1,1)模型的基础上进行改进,从而建立起营房室内有害气体污染水平预测模型。通过对预测模型进行检验,证实营房室内有害气体污染预测模型能较好的预测营房室内有害气体污染水平的发展变化趋势,模型的建立是成功的。