Ni-Zn铁氧体粉末的溶胶-凝胶合成及微波性能

以硝酸铁、硝酸镍、硝酸锌、柠檬酸和氨水为原料,用溶胶-凝胶法合成了不同组成的Ni-Zn铁氧体粉末。利用热分析、X射线衍射等手段研究了干凝胶热分解行为。利用网络分析仪对铁氧体粉末的电磁性能进行了表征,考察了铁氧体的组成与其电磁性能之间的关系。结果表明,溶胶-凝胶法合成的铁氧体粉末的μ″值随测试频率的提高和Ni-Zn铁氧体中锌含量的增加而减小。     

几何内蕴量对拉伸模具工作面力学性能的影响

曲率、度规不变量、凸凹性等几何内蕴量的不均匀分布直接影响模具的力学性能。本文研究了曲率与变形能、曲率与摩擦耗损功、度规不变量与热辐射、凸凹分布与辐射热通量等几何内蕴量与力学量之间的关系。结果表明:复杂曲面表面高斯曲率的不连续分布将导致表面的变形能、摩擦耗损功出现相应的不连续分布;型面上沿拉伸方向截面线的法曲率越小,摩擦耗损功越大;型面上的热通量会随着拐点数量的增加而增加。这些结果为模具表面优化设计提供了新的理论依据。     

一种新的基于小波域的灰度水印嵌入算法

数字水印技术作为数字产品版权保护的一项新技术,已受到越来越多的关注.为保证水印的鲁棒性,利用人类的视觉特性,提出一种基于离散小波变换的数字水印技术,并给出了攻击分析.分析中,采用灰度图像作为数字水印,使其具有二维信号可视化的优点.实验表明,该算法能够经受住噪声、高斯滤波、压缩、直方图均衡化、增加对比度等的处理,具有较强的鲁棒性,是一种行之有效的水印嵌入方法.     

2A12铝合金焊接接头超声冲击处理前后拉伸性能分析

为克服铝合金薄板焊接接头强度偏低、韧性不足的缺点,用ER5356焊丝对不同厚度的2A12铝合金板材进行了手工氩弧焊接,并采用超声冲击处理对焊接接头进行全覆盖强化处理。采用金相显微镜观察了处理和未处理焊接接头的显微组织结构,对接头的力学性能进行了测试分析,分析了超声冲击处理改善2A12铝合金焊接接头力学性能的机理。结果表明：铝合金焊接接头经超声冲击强化处理后,6 mm和4 mm厚板材对接接头的抗拉强度分别提高了17.4%和23.7%,延伸率分别提高了28%和44%,焊缝表层组织得到明显细化。分析认为：晶粒大幅细化、组织致密化和缺陷减少,是超声冲击处理改善铝合金焊接接头抗拉伸性能的主要原因。     

不同含水量超细钛酸钡电流变液性能的研究

采用溶胶-凝胶的方法,通过高温烧结得到了超细钛酸钡(BaTiO3)粉体,烧结产物经SEM、XRD等表征手段对粉体的形貌和晶型进行分析。采用卡尔-费休法测定了配制的电流变液中的含水量,讨论了不同含水量对钛酸钡的电流变性能的影响。结果表明,含水钛酸钡ER液在含水量为117．2μg／g时,屈服应力、表观粘度和漏电流密度达到最大值;要使含水钛酸钡ER液具有一定的ER效应,且在其实验仪器测试范围内(电场强度最大可达2．5kV／mm;漏电流最大可达10μA)具有电流变效应,含水量应小于或等于88．1μg／g。     

Effect of fusion welding processes on tensile properties of armor grade,high thickness,non-heat treatable aluminium alloy joints

AA5059 is one of the high strength armor grade aluminium alloy that finds its applications in the military vehicles due to the higher resistance against the armor piercing (AP) threats. This study aimed at finding the best suitable process among the fusion welding processes such as gas tungsten arc welding (GTAW) and gas metal arc welding (GMAW) by evaluating the tensile properties of AA5059 aluminium alloy joints. The fracture path was identified by mapping the low hardness distribution profile (LHDP) across the weld cross section under tensile loading. Optical and scanning electron microscopies were used to characterize the microstructural features of the welded joints at various zones. It is evident from the results that GTAW joints showed superior tensile properties compared to GMAW joints and this is primarily owing to the presence of finer grains in the weld metal zone (WMZ) and narrow heat-affected zone (HAZ). The lower heat input associated with the GTAW process effectively reduced the size of the WMZ and HAZ compared to GMAW process. Lower heat input of GTAW process results in faster cooling rate which hinders the grain growth and reduces the evaporation of magnesium in weld metal compared to GMAW joints. The fracture surface of GTAW joint consists of more dimples than GMAW joints which is an indication that the GTAW joint possess improved ductility than GMAW joint.     

酚醛-石英混杂纤维增强苯并噁嗪复合材料高温失效特征

通过模压工艺制备了酚醛-石英混织纤维增强苯并噁嗪复合材料(P-Q/BZ)试样,考察了其力学性能、烧蚀性能和耐冲刷性能,分析了该试样在高温环境中的主要失效特征,研究其在高温环境中的适用性。结果表明,未经热处理的P-Q/BZ试样平均弯曲强度、弯曲模量和层间剪切强度分别为283 MPa、10.8 GPa和22.6 MPa;经300℃,N_2处理15 min后,试样均匀膨胀,厚度增加22%,弯曲强度、弯曲模量和层间剪切强度分别下降58%、41%和58%;在氧乙炔焰的平均质量烧蚀率和线烧蚀率分别为0.048 4 g/s和-0.081 mm/s,烧蚀后试样宏观不分层,表面炭层微观分层严重,酚醛纤维热解炭、树脂基体热解炭、熔融石英纤维以及碳硅氧化产物相互分离;该试样耐冲刷能力差,在发动机尾焰烧蚀平台模拟的热-力耦合环境中的质量损失率高达59%。P-Q/BZ复合材料需要解决热解膨胀问题,进一步提高抗冲刷性能。     

Multifunctional A356 alloy/ PKSAnp composites: Microstructure and mechanical properties

Mechanical properties and microstructure of multifunctional composites produced with palm kernel shell ash nanoparticle (PKSAnp)-A356 alloy composites was studied. The composites were produced using Double layer feeding stir casting method (DLF-SCM) by adding 1 wt%‒4 wt.% PKSAnp. The microstructure, density, electrical and mechanical properties were determined. The results shows that there was a uniform distribution of the PKSAnp in A356 alloy. The mismatch at the interface between the PKSAnp and A356 alloy was 4.26%. Improvement of 30.47%, 41.91%, 49.52%, 40.90% and 65.09% were obtained for hardness values, tensile, yield strength, %elongation and impact energy at 4 wt% PKASnp. The work has established that the developed composites can be used for multifunctional applications where combination of toughness and strength is vital.     

室内装饰织物燃烧特性研究

室内装饰织物因其容易点燃、燃烧速度快、蔓延迅速等燃烧特性,对室内火灾的发展蔓延及火灾危害都有重要影响。运用锥形量热仪对棉麻、涤纶、帆布、泡纱、条绒等5种室内装饰织物的燃烧性能进行了实验研究,测量了室内装饰织物在不同热辐射条件下的燃烧特性,并对实验数据进行图像拟合,通过具体的实验数据和图像分析比较了5种室内装饰织物在不同热辐射条件下的点燃时间、热释放速率、质量损失速率、比消光面积及CO生成量。最后得出了各种织物的火灾危险性相对大小。     

RTM工艺整体成型复合材料连接裙轴压性能

整体成型的固体火箭发动机复合材料连接裙有助于连接裙的减重及其使用性能的提高。本文采用RTM工艺制备出了全复合材料整体连接裙并对其进行了轴压承载性能考核。试验结果表明,RTM工艺整体成型的复合材料连接裙质量均匀,在设计载荷作用下,连接裙的轴向应变远小于0.5%的复合材料许用应变指标,连接裙的轴向表观结构刚度为40.9GPa。