| 硫二甘醇及其相关氧化产物的硅烷化衍生反应条件优化及应用 |
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| 引用本文： | 吴晓飞 周世坤 刘景全. 硫二甘醇及其相关氧化产物的硅烷化衍生反应条件优化及应用[J]. 防化研究, 2007, 0(1): 20-23 |
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| 作者姓名： | 吴晓飞 周世坤 刘景全 |
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| 摘 要： | 研究了衍生气相色谱法测定芥子气的降解产物硫二甘醇、硫二甘醇亚砜和硫二甘醇砜的方法，并对影响衍生反应的溶剂、温度、时间和衍生试剂用量进行了优化，该法操作简便、灵敏度高。
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| 关 键 词： | 硅烷化衍生方法 硫二甘醇 硫二甘醇亚砜 硫二甘醇砜 气相色谱 |
| 修稿时间： | 2006-01-08 |
Application and optimization of silylation reaction for the determination of thiodiglycol and oxidation products |
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| Wu Xiaofei, Zhou Shikun, Liu Jingquan. Application and optimization of silylation reaction for the determination of thiodiglycol and oxidation products[J]. , 2007, 0(1): 20-23 |
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| Authors: | Wu Xiaofei Zhou Shikun Liu Jingquan |
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| Abstract: | A method for determination of thiodiglycol, thiodiglycol sulphoxide and thiodiglycol sulphone by gas chromatography after silylated derivatives are studied. The detection conditions are optimized. The method is convenient and sensitive. |
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| Keywords: | silylation thiodiglycol thiodiglycol sulphoxide thiodiglycol sulphone GC |
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