两个含磷、氮化合物的EI-MS分析

采用气相色谱一质谱联用技术对二异丙氨基甲基膦酸乙基酯和N,N-双（2-甲基膦酸乙基酯乙基）甲基胺2个合成样品进行了分析,比较深入地研究了2个化合物的质谱裂解规律,并推断了样品中相关杂质的结构。     

化学毒剂相关化合物的液相色谱－质谱分析

综述了1990年以来采用液相色谱－质谱联用技术（LC－MS）分析化学毒剂相关化合物的应用现状和发展趋势。     

毒剂样品H90中芥子气和路易氏气的分析研究

运用气相色谱－质谱（ＧＣ－ＭＳ）分析测定了毒剂样品Ｈ９０中的芥子气和路易氏气,并用气相色谱－红外光谱（ＧＣ－ＦＴＩＲ）联用这一分离分析手段,研究了上述毒剂的红外吸收特性,为其进一步鉴定提供了重要依据。     

液相色谱-质谱法测定2-氯乙烯胂酸

研究了用液相色谱-质谱两种电离技术测定路易氏剂1的降解产物2-氯乙烯胂酸,比较了在不同流动相中该化合物的响应情况,并且利用源内CID技术获得了丰富质谱碎片,对所鉴定的碎片进行了解释,用选择离子检测得到该化合物的检测限在APCI电离技术中为9ng,在ESI电离技术中为4ng．     

路易氏剂衍生物的气相色谱-质谱研究

用一种单巯基化合物1-巯基丙烷和三种双巯基化合物1,3-二巯基丙烷、2,3-二巯基丙醇、3,4-二巯基甲苯经亲核取代反应将路易氏剂衍生为挥发性较好的二硫砷化合物,用GC-MS鉴定了这些化合物的结构,并讨论了分子离子的碎裂方式及个别碎片的来源．     

汽油燃烧产物GC-MS分析的萃取剂研究

应用色谱/质谱联用技术对提取93#汽油燃烧烟尘及残留物特征组分的五种萃取剂进行了对比研究。在确保制样过程中汽油组分提取量尽可能一致性的条件下,以提取出的有机特征组分的种类和相对峰面积为标准,利用总离子流色谱图和质量色谱图定性分析了五种萃取剂的萃取效果。     

质谱技术在火灾物证鉴定中的应用

随着火灾原因的多样化、复杂化，应用准确、高效的现代化仪器分析的方法鉴定火灾原因日益重要。简述了质谱相关技术，如气相色谱／质谱技术（GC／MS），串联质谱技术（MS／MS）等在火灾物证鉴定中的应用。     

一个未知样品中溴化新斯的明的鉴定

用质和红外光谱技术鉴定了一个未知样品中的溴化新斯的明,研究发现这个化合物在通过GC系统时极易热分解,因此,GC／MS的测定结果不能区分新斯的明的溴盐和碘盐。直接进样质谱测试解决了这个问题。红外光谱支持质谱的结论,并提供了样品含大量的信息。     

衍生化气相色谱-质谱法鉴定三乙胺及其相关化合物

用气相色谱－质谱法对三乙醇胺及其相关化合物进行了分析研究,探讨了它们的原体和硅烷化两种情况下电子轰击电离（ＥＩ）的质谱规律,并对待测化合物的色谱保留数据进行了研究。在通常情况下,各种待测化合物用ＳＥ－５４色谱柱能有效地分离,三乙醇胺及基相关化合物在未衍生物之前峰形较差,硅烷化后峰形变尖锐,化合物之间更容易分辨。     

化学毒剂相关化合物的电喷雾及大气压化学电离质谱研究

采用电喷雾质谱（ESI－MS）技术对化学毒剂相关化合物的测定进行了优化。初步将大气压化学电离质谱（APCI－MS）用于测定化学毒剂相关化合物。     

Helping hands: civil–military cooperation and Italy's military operation abroad

In the Post-Bipolar Era the growing complexity of the military operations requires a new approach for the resolution of international crises. Since the end of the Cold War, peace support operations (PSO) have become the mainstay and principal occupation of most Western armies. At the same time, Italy has been one of the most important actors in such an area. The article focuses on the cooperation between military and civil components (a process called CIMIC) as a key variable in the Italian PSOs. We will analyse in detail the main lessons learned from past military interventions as well as the general context in which new tendencies are taking place. The maintaining of a minimum security frame becomes essential to fulfil activities ‘collateral’ to the mission: reconstructing services and infrastructure, food distribution, water and medication, law and order, de-mining, training of local forces, and supporting local institutions. These are the main tasks to obtain thrust and support from the population.     

Terrorism,insurgency, kidnapping,and security in Africa's energy sector

Energy continues to serve as the bedrock of modern economies and the main driver of modern society. For Africa, the production and supply of energy resources such as crude oil, natural gas, uranium, coal, biomass, biofuels and other renewables are an important source of employment, rents, taxes, royalties and profits. This sector brings in several tens of billions of dollars of revenue annually. The production and delivery of such resources, however, depend on critical infrastructures such as pipelines, refineries, processing plants, terminals, rigs, electrical energy pylons, substations, pump stations, vessels, and tankers. These infrastructures have been attacked by terrorists, insurgents, vandals and saboteurs, all of whom see them as targets against which to register their grievances and extract concessions from the state. This paper is a chronological account of some of the documented incidents of terrorism, insurgency, kidnapping, destruction, sabotage, and human casualties suffered in the oil and gas sectors in Africa between 1999 and 2012. It is based on data extracted from the databases of the RAND Database of World Terrorism Incidents and the University of Maryland's Global Terrorism Database (GTD).     

Tacit support for terrorism: The rapprochement between the USSR and Palestinian guerrilla organizations following the 1967 war

This article demonstrates the inconsistent and wavering Soviet attitude towards national liberation movements in general and the Palestinian organizations in particular. Until the late 1960s, the Soviets viewed these organizations with suspicion, hesitating to engage in political dialogue with them. However, in the 1970s, political and military events in the region, as well as modifications in the Kremlin's Cold War strategies, led to a general shift towards the Middle East in Soviet foreign policy. Soviet leaders showed increased willingness to provide certain Palestinian organizations with arms with which to conduct terrorist activities against Israeli, pro-Israeli, Jewish and Western targets. The article explores the complex relations between Palestinian organizations and the USSR in the field of international terror. The study also exposes and analyzes the nature and content of Soviet–Palestinian arms dialogues and transactions. It provides clear evidence that Soviet policymakers and other luminaries were fully informed of, and sometimes directly involved in, these transactions and dialogues at the highest levels.     

A1 Qaeda and the radical Islamic challenge to western strategy

The September 11 global crisis prompted by the attacks on the World Trade Center and the Pentagon raises major questions concerning the nature and trajectory of terrorism in the post-Cold War global order. Hitherto, terrorism has been largely debated by analysts at the level of nation states. Terrorist and insurgent movements have also been largely anchored in nationalist and ethnic power bases even when they have sought to mobilise a transnational ideological appeal on religious or class grounds. There have been a few exceptions to this pattern such as the alliance between the German Baader-Meinhof group and the Japanese Red Army Faction, but even such international alliances as this did not, until at least the 1980s, presage anything like a global terrorist network necessitating a global strategic response. This study examines terrorism and global strategic responses.     

Helping hands: external support for the KNU insurgency in Burma

This article analyses to what extent the Burmese KNU insurgency made use of external support from states, refugees, and diasporas. Based on extensive fieldwork it is concluded that support from neighbouring states and refugees has for years kept the Karen rebellion alive. Western countries perceived forms of resistance to the illegitimate Burmese regime as just and have therefore played a crucial role in the continuation of conflict in Karen State. It is important that policymakers and donors as well as executing organizations continue to reflect critically on the way they exercise their work.     

Reviews

Douglas S. Derrer, We Are All the Target: A Handbook of Terrorism Avoidance and Hostage Survival. Annapolis, MD: US Naval Institute Press, 1992. Pp. x+135, notes, index. $14.95. ISBN 01–55750–150–5

Ian Knight, Zulu: Isandlwana and Rorke's Drift, 22–23 January 1879. London: Windrow & Greene, 1992. Pp.136, 150 illus., incl 8 colour plates, maps, biblio. £35. ISBN 1–872004–23–7

Ian Knight, By the Orders of the Great White Queen: Campaigning in Zululand through the Eyes of the British Soldiers, 1879. London: Greenhill Books and Novato: Presidio Press, 1992. Pp. 272, 17 illus., 1 map. £18.95. ISBN 1–85367–122–3

Manfried Rauchensteiner and Erwin A. Schmidl (eds.), Formen des Krieges: vom Mittelalter zum ‘Low‐intensity’ Conflict’. Graz : Verlag Styria, 1991. Pp.208. DM35. ISBN 3–22–12139–7

Harold J. Kearsley, Maritime Power and the Twenty‐First Century. Dartmouth: Dartmouth Publishing Company, Limited, 1992. Pp.xv + 203, 13 diagrams, index. £32.50. ISBN 1–85521–288–9     

基于GTST-DMLD-ESD的装备RMS建模仿真

装备的RMS是装备的重要设计参数,是影响战备完好和保障能力的关键因素.引入GTST-DMLD作为主要建模工具,建立起装备系统的RMS描述模型,以ESD为补充和扩展,对维修过程进行建模.并以GTST-DMLD-ESD模型作为装备RMS仿真的核心,对装备RMS仿真模型的总体框架进行了研究,并对各模块进行了较为详细的探讨.     

Cyber sheiks and grassroots jihadis: the war in Syria and the devolution of the Bosnian Salafi communities

ABSTRACT

What was the scope of the Bosnian jihadi participation in the war in Syria? Did the Bosnian volunteers tend to join one particular faction? Why did the Bosnian youngsters decide to join the holy war in the Levant? Was this an organized and hierarchical process or was this a grassroots movement? Last, were all the Salafis in Bosnia supportive of this dynamic or did this process cause internal frictions? These are some of the questions that this research will try to answer.