高pH条件纳米Fe_3O_4催化H_2O_2分解去除水中4-氯酚

为了克服非均相fenton催化反应中溶液初始pH过低的缺点,开展了pH=5时Fe3O4/H2O2体系催化氧化去除水中4-氯酚实验。试验结果表明:制备的铁氧化物为纯Fe3O4,具有反尖晶石八面体结构。纳米Fe3O4能够高效催化H2O2分解氧化水中的4-氯酚,反应180 min后4-氯酚的去除率达到96.8%。当催化剂投量小于2.0 g/L,4-氯酚的去除率随着催化剂投量的增加而升高;当催化剂投量大于2.0 g/L,去除率会随着投量的增加而降低。随着H2O2投量的增加,4-氯酚的去除率先升高后降低。溶液的初始pH对4-氯酚的去除影响较大,pH越低,去除速率和效率越高。重复使用5次以后,纳米Fe3O4仍然保持较高的催化活性。     

Statistical analysis for masked system life data from Marshall‐Olkin Weibull distribution under progressive hybrid censoring

This paper considers the statistical analysis of masked data in a series system, where the components are assumed to have Marshall‐Olkin Weibull distribution. Based on type‐I progressive hybrid censored and masked data, we derive the maximum likelihood estimates, approximate confidence intervals, and bootstrap confidence intervals of unknown parameters. As the maximum likelihood estimate does not exist for small sample size, Gibbs sampling is used to obtain the Bayesian estimates and Monte Carlo method is employed to construct the credible intervals based on Jefferys prior with partial information. Numerical simulations are performed to compare the performances of the proposed methods and one data set is analyzed.     

One-step synthesis of FeO(OH) nanoparticles by electric explosion of iron wire underwater

In this study,we investigated electric explosion of iron wire in distilled water with different energy input adjusted by charging voltage.The as-prepared samples were characterized by X-ray diffraction (XRD),scanning electron microscopy (SEM),transmission electron microscopy (TEM) and X-ray photoelectron spectroscopy (XPS),showing the presence of iron and multiple iron-based compounds oxides with contents influenced by the experimental conditions.In particular,pure FeO(OH) nanoparticles were obtained using electric explosion of iron wire with energy input of 1125 J at charging voltage of 15 kV.Analysis of discharge current and resistive voltage data indicate that the high energy input induced by strong plasma discharge at high charging voltage is a key factor to form FeO(OH).This study presents a one-step method to synthesize FeO(OH) nanoparticles using electric explosion of iron wire.     

基于遗传算法的无线通信节点部署优化策略

根据无线通信节点部署过程中网络受到区域环境影响和电波传播损耗等实际问题,建立了考虑区域影响的信号衰减模型和无线通信网络覆盖模型,提出了一种综合考虑网络覆盖和通信干扰的优化部署策略。该策略采用了加速遗传算法,大大降低了计算量。基于该优化策略,通过仿真实验得到了特定区域的最优通信节点数和节点部署位置图。     

消防部队基层指挥员作战指挥能力评估研究

通过建立消防部队基层指挥员作战指挥能力评估模型,采用模糊综合评判和层次分析法(AHP),对基层指挥员作战指挥能力给出了较为精确的计量,可以了解掌握基层指挥员自身实力和存在不足,也为上级用人提供依据.     

中庭内步梯在火灾疏散中的应用探讨

对中庭内步梯在火灾情况下人员紧急疏散的使用进行了探讨,提出了使用水幕减弱火灾辐射危害的措施,并运用火灾危险分析方法进行了论述。     

论武警学院的双语教学

双语教学已成为高校教育改革的一大焦点。结合开展双语教学工作 ,考虑到各方面因素 ,提出了武警学院开展双语教学的具体措施。     

卫星通信抗干扰技术综述

卫星在现代战争中发挥着举足轻重的作用,提高卫星通信的抗干扰能力具有非常重要的意义.通过分析卫星通信系统面临的各种干扰类型,综述了现有卫星通信系统常用的抗干扰技术的原理、特点和国外的发展现状,包括天线抗干扰技术、扩频技术、星上处理技术等.讨论了卫星通信抗干扰技术研究的发展方向和今后值得进一步研究的问题.     

水面舰艇攻势防御的效能评估及优势论证

进攻是最好的防守。针对水面舰艇攻势防御问题,对水面舰艇攻势防御的概念及使用前提进行了讨论,通过与守势防御的比较,从理论上对攻势防御的优势进行了论证。最后,根据论证结果、数据仿真及作战实际,给出了攻势防御的使用原则。