液相色谱-质谱法测定2-氯乙烯胂酸

研究了用液相色谱-质谱两种电离技术测定路易氏剂1的降解产物2-氯乙烯胂酸,比较了在不同流动相中该化合物的响应情况,并且利用源内CID技术获得了丰富质谱碎片,对所鉴定的碎片进行了解释,用选择离子检测得到该化合物的检测限在APCI电离技术中为9ng,在ESI电离技术中为4ng．     

Ti含量对Ti-B4C-C体系自蔓延高温合成的影响

以14Ti+3B4C+5C为基础反应体系,通过热力学分析及静态燃烧合成实验研究了钛含量对该体系SHS反应的绝热温度、反应速度和产物致密度的影响.研究表明,Ti含量适当增加,能够使反应速度加快、产物致密度提高.当Ti过量16%(摩尔分数)时,体系的绝热温度仍高达3 193K,反应速度最快,产物的致密度也较高.     

PS／2键盘接口在单片机中的应用研究

PS/2键盘接口由于采用标准PS/2协议通信,易于控制,在嵌入式系统中有良好的应用前景.针对如何使用这种接口,介绍了其物理接口及通信协议,重点对工作时序和部分命令字进行了说明.在应用中,给出了PS/2键盘与单片机的接口电路及通信方案,并提供相应的接口通信程序.     

群体性事件中的思想工作策略研究

在群体性事件发生后,思想工作具有重要的阻断冲突升级的功能。要阻断群体性事件的升级,就要着眼于从警示教育、心理干预、思想沟通、信息调控等方面来建设阻断群体性事件升级的思想工作应对机制。     

团体沙盘游戏疗法在大学新生适应问题干预中的应用

团体沙盘游戏疗法是沙盘疗法的一个组成部分,因其独特的教育和治疗功能,特别适合大学新生适应性训练。本文针对大学新生自我认识、情绪管理、人际关系等适应性问题,利用团体沙盘游戏进行了干预研究,取得了很好的教育效果。     

匈牙利法的末段两层火力反TBM目标分配优化

介绍了匈牙利法解决Assignment Problem的基本原理,对匈牙利法解决指派问题的解题步骤和特殊情况进行了说明。在给出末段两层火力防御TBM的目标分配原则的基础上,阐述了相关概念,改进了匈牙利法运用方式,并建立了目标分配模型。最后通过实例的解算,证明了该方法应用于末段两层火力防御TBM目标分配中的可行性,为末段协同反TBM的目标分配提供了一种有效的算法。     

改进的拉格朗日松弛数据关联算法

在多传感器多目标跟踪领域中,当传感器为被动式的,传统的多维分配算法利用拉格朗日松弛算法求解.拉格朗日乘子更新一般用次梯度方法,但每次迭代都要进行多次极小化运算来求对偶解,导致实时性差.针对这个问题,提出了一种改进的基于拉格朗日松弛的数据关联算法,通过代理修正次梯度方法更新拉格朗日乘子,并在允许时间内获得近似解.仿真实验...     

基于不确定度的专家评价综合方法

针对群决策中专家评价信息的综合处理问题,应用多位专家评价的评价样本不确定度,提出了基于不确定度的数据综合处理方法。该方法能够有效应用于群决策问题,尤其是参与决策人员(专家)较多时,出现专家相对权重可信度不明确而导致评价准确度低的问题,科学地简化了群决策中专家权重的确定过程,便于应用,具有坚实的理论依据和应用价值。通过算例分析,该方法的有效性得到了验证。     

Study of high-speed-impact-induced conoidal fracture of Ti alloy layer in composite armor plate composed of Ti-and Al-alloy layers

In order to understand the mechanism of conoidal fracture damage caused by a high-speed fragment-simulating projectile in titanium alloy layer of a composite armor plate composed of titanium- and aluminum-alloy layers, the ballistic interaction process was successfully simulated based on the Tuler-Butcher and GISSMO coupling failure model. The simulated conoidal fracture morphology was in good agreement with the three-dimensional industrial-computed-tomography image. Further, three main damage zones (zones I, II, and III) were identified besides the crater area, which are located respectively near the crater area, at the back of the target plate, and directly below the crater area. Under the high-speed-impact conditions, in zone II, cracks began to form at the end of the period of crack formation in zone I, but crack formation in zone III started before the end of crack formation in zone II. Further, the damage mechanism differed for different stress states. The microcracks in zone I were formed both by void connection and shear deformation. In the formation of zone I, the stress triaxiality ranged from-2.0 to-1.0, and the shear failure mechanism played a dominant role. The microcracks in zone II showed the combined features of shear deformation and void connection, and during the for-mation process, the stress triaxiality was between 0 and 0.5 with a mixed failure mode. Further, the microcracks in zone III showed obvious characteristics of void connection caused by local melting. During the zone III formation, the triaxiality was 1.0-1.9, and the ductile fracture mechanism was dominant, which also reflects the phenomenon of spallation.     

Damage modeling of ballistic penetration and impact behavior of concrete panel under low and high velocities

This work presents a numerical simulation of ballistic penetration and high velocity impact behavior of plain and reinforced concrete panels. This paper is divided into two parts. The first part consists of numerical modeling of reinforced concrete panel penetrated with a spherical projectile using concrete damage plasticity (CDP) model, while the second part focuses on the comparison of CDP model and Johnson-Holmquist-2 (JH-2) damage model and their ability to describe the behavior of concrete panel under impact loads. The first and second concrete panels have dimensions of 1500 mm × 1500 mm × 150 mm and 675 mm × 675 mm × 200 mm, respectively, and are meshed using 8-node hexahedron solid elements. The impact object used in the first part is a spherical projectile of 150 mm diameter, while in the second part steel projectile of a length of 152 mm is modeled as rigid element. Failure and scabbing characteristics are studied in the first part. In the second part, the com-parison results are presented as damage contours, kinetic energy of projectile and internal energy of the concrete. The results revealed a severe fracture of the panel and high kinetic energy of the projectile using CDP model comparing to the JH-2 model. In addition, the internal energy of concrete using CDP model was found to be less comparing to the JH-2 model.