烧结助剂对热压SiCw/Si3N4复合材料性能的影响

本文通过热压的方法分别制得以Ｙ２Ｏ３－Ａｌ２Ｏ３和Ｙ２Ｏ３－Ｌａ２Ｏ３为烧结助剂的ＳｉＣｗ／Ｓｉ３Ｎ４陶瓷基复合材料，对比了采用不同种类及含量的烧结助剂的ＳｉＣｗ／Ｓｉ３Ｎ４复合材料的性能结果，发现烧结助剂的种类及含量对ＳｉＣｗ／Ｓｉ３Ｎ４复合材料的弯曲强度和断裂韧性有明显的影响，对高温弯曲强度的影响尤为显著。     

金属/SiO2复合气凝胶催化剂对一氧化碳氧化的催化

采用溶胶－凝胶法和超临界干燥法制备了Ｃｕ／ＳｉＯ２ 和Ｃｏ／ＳｉＯ２ 气凝胶催化剂， 对其结构和形貌进行了ＸＲＤ、ＴＥＭ 和比表面分析， 并考察了其对ＣＯ氧化的催化性能。实验结果表明， 制得的Ｃｕ／ＳｉＯ２ 和Ｃｏ／ＳｉＯ２ 气凝胶催化剂均保留了气凝胶的纳米网络和高比表面积， 活性组份均匀地分散在纳米级二氧化硅气凝胶载体中， 对ＣＯ的氧化均表现出高的催化活性。     

用溶胶-凝胶法制备碳纤维三维编织物增强氧化铝基复合材料的研究

本文研究了溶胶－凝胶（Ｓｏｌ－ｇｅｌ）法制备碳纤维三维编织物增强氧化铝（Ａｌ２Ｏ３）基复合材料的成型工艺及其力学性能，研究了两种主要起始物Ａｌ（ＮＯ３）３、ＡｌＣｌ３配制的氧化铝溶胶对复合材料成型工艺和力学性能的影响。分别以Ａｌ（ＮＯ３）３和ＡｌＣｌ３为起始物，制备得到Ⅰ＃、Ｉ＃复合材料。研究表明，以Ａｌ（ＮＯ３）３为起始物配制的溶胶粘度较小，利于材料的致密化。经过溶胶浸渍、凝胶、裂解１３个周期后，Ⅰ＃材料的密度和室温三点弯曲强度分别为１．８６ｇ／ｃｍ３和１４５．２ＭＰａ，而ＩＩ＃材料的密度和室温三点弯曲强度分别为１．６３ｇ／ｃｍ３和１０４．１ＭＰａ，材料均呈典型的韧性断裂模式。用扫描电子显微镜（ＳＥＭ）观察试样的断口形貌，发现断口表面有大量的纤维拔出，纤维表现了较好的增韧效果。     

Ag2O 添加的YBa2 Cu3O7-δ超导材料的超导性能

用固态反应法按分子式ＹＢａ２Ｃｕ２．７Ａｇ０．３Ｏ７－δ（简称ＹＢＣＡＯ）制备了样品，利用Ｘ射线衍射，Ｒ－Ｔ曲线及扫描电镜ＳＥＭ研究了Ａｇ对于ＹＢＣＯ超导性能的影响。实验结果表明：晶粒得以细化，ＹＢＣＯ超导性能的稳定性有所增强。本文对结果进行了讨论。     

MEASUREMENT OF PLASMA POTENTIAL USING EMISSIVE PROBE IN A MAGNETIC MIRROR

ＭＥＡＳＵＲＥＭＥＮＴＯＦＰＬＡＳＭＡＰＯＴＥＮＴＩＡＬＵＳＩＮＧＥＭＩＳＳＩＶＥＰＲＯＢＥＩＮＡＭＡＧＮＥＴＩＣＭＩＲＲＯＲＺｈａｎｇＪｉａｎｄｅ（ＤｅｐａｒｔｍｅｎｔｏｆＡｐｐｌｉｅｄＰｈｙｓｉｃｓ,ＮＵＤＴ,Ｃｈａｎｇｓｈａ,４１００７３）Ｆａ...     

AN UNIFIED METHOD AND THEORY FOR GRAMMAR DESIGN OF A CLASS OF CONTEXT-SENSITIVE LANGUAGES

ＡＮＵＮＩＦＩＥＤＭＥＴＨＯＤＡＮＤＴＨＥＯＲＹＦＯＲＧＲＡＭＭＡＲＤＥＳＩＧＮ　ＯＦＡＣＬＡＳＳＯＦＣＯＮＴＥＸＴ－ＳＥＮＳＩＴＩＶＥＬＡＮＧＵＡＧＥＳＬｉＺｈｏｕｊｕｎ;ＣｈｅｎＨｕｏｗａｎｇ;ＬｉＫａｎ（ＤｅｐａｒｔｍｅｎｔｏｆＣｏｍｐｕｔｅｒ...     

A COMPLEX OF TWO OPTIMIZATION IDEAS IN OPTICAL AUTOMATIC DESIGN

ＡＣＯＭＰＬＥＸＯＦＴＷＯＯＰＴＩＭＩＺＡＴＩＯＮＩＤＥＡＳＩＮＯＰＴＩＣＡＬＡＵＴＯＭＡＴＩＣＤＥＳＩＧＮＷａｎｇＹｏｎｇｚｈｏｎｇ（ＤｅｐａｒｔｍｅｎｔｏｆＡｐｐｌｉｅｄＰｈｙｓｉｃｓ,ＮＵＤＴ,Ｃｈａｎｇｓｈａ,４１００７３）Ａｂｓｔｒａｃｔ：...     

(G2-continuous) SHAPE PRESERVING CUBIC INTERPOLATION SPLINE CURVE

（Ｇ~２－ｃｏｎｔｉｎｕｏｕｓ）ＳＨＡＰＥＰＲＥＳＥＲＶＩＮＧＣＵＢＩＣＩＮＴＥＲＰＯＬＡＴＩＯＮＳＰＬＩＮＥ　ＣＵＲＶＥＦａｎｇＫｕｉ（ＤｅｐａｒｔｍｅｎｔｏｆＳｙｓｔｅｍＥｎｇｉｎｅｅｒｉｎｇａｎｄＭａｔｈｅｍａｔｉｃｓ,ＮＵＤＴ,Ｃｈａｎｇｓｈ?..     

RESEARCH ON TECHNOLOGY AND SYSTEM FOR ON-LINE MEASUREMENT OF SURFACE ROUGHNESS IN ULTRA-PRECISION MACHINING

ＲＥＳＥＡＲＣＨＯＮＴＥＣＨＮＯＬＯＧＹＡＮＤＳＹＳＴＥＭＦＯＲＯＮ－ＬＩＮＥＭＥＡＳＵＲＥＭＥＮＴＯＦＳＵＲＦＡＣＥＲＯＵＧＨＮＥＳＳＩＮＵＬＴＲＡ－ＰＲＥＣＩＳＩＯＮＭＡＣＨＩＮＩＮＧＬｕＨａｉｂａｏ;ＷａｎｇＹａｏｋｅ;ＺｈｕＪｉｇｕｉ;Ｚｈｏ...     

STUDY ON REALISTIC TECHNOLOGY OF CONDITION MONITORING AND FAULT DIAGNOSTIC SYSTEM FOR SHIPPING POWER DEVICES

ＳＴＵＤＹＯＮＲＥＡＬＩＳＴＩＣＴＥＣＨＮＯＬＯＧＹＯＦＣＯＮＤＩＴＩＯＮＭＯＮＩＴＯＲＩＮＧＡＮＤＦＡＵＬＴＤＩＡＧＮＯＳＴＩＣＳＹＳＴＥＭＦＯＲＳＨＩＰＰＩＮＧＰＯＷＥＲＤＥＶＩＣＥＳＷｅｎＸｉｓｅｎ;ＬｉＹｕｅ;ＴａｎｇＢｉｎｇｙａｎｇ（Ｄｅｐ...     

Formation and characterization of core-shell CL-20/TNT composite prepared by spray-drying technique

The core-shell 2,4,6,8,10,12-Hexanitro-2,4,6,8,10,12-hexaazaisowurtzitane/2,4,6-Trinitrotoluene (CL-20/TNT) composite was prepared by spray-drying method in which sensitive high energy explosive (CL-20) was coated with insensitive explosive (TNT). The structure and properties of different formulations of CL-20/TNT composite and CL-20/TNT mixture were characterized by scanning electron microscopy (SEM), Transmission electron microscopy (TEM), Laser particle size analyzer, X-ray photoelectron spectroscopy (XPS), X-ray diffraction (XRD), differential scanning calorimetry (DSC), impact sensitivity test and detonation performance. The results of SEM, TEM, XPS and XRD show that ϵ-CL-20 particles are coated by TNT. When the ratio of CL-20/TNT is 75/25, core-shell structure is well formed, and thickness of the shell is about 20–30 nm. And the analysis of heat and impact show that with the increase of TNT content, the TNT coating on the core-shell composite material can not only catalyze the thermal decomposition of core material (CL-20), but also greatly reduce the impact sensitivity. Compared with the CL-20/TNT mixture (75/25) at the same ratio, the characteristic drop height of core-shell CL-20/TNT composite (75/25) increased by 47.6% and the TNT coating can accelerate the nuclear decomposition in the CL-20/TNT composites. Therefore, the preparation of the core-shell composites can be regarded as a unique means, by which the composites are characterized by controllable decomposition rate, high energy and excellent mechanical sensitivity and could be applied to propellants and other fields.     

气氧/煤油发动机水冷推力室壁热分析

针对气氧／煤油地面试验发动机的热防护问题，采用非定常三维壁温分布模型为主体的分析模型，对槽道式水冷推力室壁温特性进行了计算分析。燃气流与冷却水流采用一维流动模型计算。应用有限差分方法确定了燃气与室壁的换热热流、推力室壁温分布，给出了壁温随时间变化的规律，讨论了冷却水流量对壁温的影响。     

在单晶硅片上直接电化学沉积制备镍反opal光子晶体

采用电化学沉积工艺直接向组装在单晶硅片上的聚苯乙烯胶体晶体中填充金属Ni,成功制备了Ni的反opal光子晶体。采用线性扫描伏安法研究了单晶硅表面的化学刻蚀对Ni的电化学沉积过程的影响,并采用扫描电子显微镜(SEM)、X射线衍射等对Ni反opal光子晶体的形貌和结构进行了观察分析,对其光学性能进行了初步研究。研究结果表明,对单晶硅片表面进行化学刻蚀有利于金属Ni的电化学沉积;在PS胶体晶体模板中电化学生长的金属Ni呈多晶状态,去除模板后形成了金属Ni的有序多孔结构。     

环氧树脂/CTBN/无机颗粒高分子合金修补剂材料的制备与性能分析

通过端羧基丁腈液态橡胶(Carboxyl Terminated Butadiene Acrylonitrile,CTBN)协同纳米Al2O3、SiO2颗粒与微米MoS2颗粒共混改性环氧树脂,制备了双组分的耐磨高分子合金修补剂材料。采用拉伸、摩擦磨损等试验及SEM等方法测试和分析了该高分子合金修补剂的拉伸强度、显微硬度等基本性能及摩擦学性能,并对其耐磨减摩机理进行了分析。结果表明:该材料的拉伸强度为42.3MPa,拉伸剪切强度为13.8MPa,显微硬度为231.1MPa,摩擦因数为0.17,耐磨性比LY12铝合金提高了50%。     

球磨时间对纳米SiO_2/Cu复合材料摩擦学性能的影响

采用球磨法与热压烧结工艺制备了添加w（n-SiO2）=1.0%的铜基纳米复合材料。通过球盘式摩擦磨损试验机测试了复合材料的摩擦磨损性能,采用排水法和场发射扫描电镜（FSEM）研究了复合材料的致密度、显微组织和磨损形貌。结果表明：球磨可提高复合材料的致密度,改善n-SiO2在铜基体中的分散均匀性;随球磨时间的增加,复合材料的动摩擦因数和磨损量先减小后增加,球磨10 h复合材料具有较低的摩擦因数和磨损量,磨损机理主要为磨料磨损。     

Preparation and property of CL-20/BAMO-THF energetic nanocomposites

A sol-gel freezing-drying method was utilized to prepare energetic nanocomposites based on 2, 4, 6, 8, 10, 12-hexanitro-2, 4, 6, 8, 10, 12-hexaazaisowurtzitane (CL-20) with 3, 3-Bis (azidomethyl) oxetane-tetrahydrofuran copolymer (BAMO-THF) as energetic gel matrix. Scanning electron microscopy (SEM), X-ray diffraction (XRD), Raman, Fourier-transform infrared spectroscopy (FT-IR) and differential thermal analyser (DTA) were utilized to characterize the structure and property of the resultant energetic nanocomposites. Compared with raw CL-20, the average particle sizes of CL-20 in CL-20/BAMO-THF energetic nanocomposites were decreased to nano scale and the morphologies of CL-20 were also changed from prismatic to spherical. FT-IR detection revealed that CL-20 particles were recrystallized in BAMO-THF gel matrix during the freezing-drying process. The thermal decomposition behaviors of the energetic nanocomposites were investigated as well. The thermolysis process of CL-20/BAMO-THF nanocomposites was enhanced and the activation energy was lower compared with that of raw CL-20, indicating that CL-20/BAMO-THF nanocomposites showed high thermolysis activity. The impact sensitivity tests indicated that CL-20/BAMO-THF energetic nanocomposites presented low sensitivity performance.     

C4ISR系统开发的仿真模型描述研究

C4ISR(Command、Control、Communication、Computer、Intelligence、Surveillance and Reconnaissance)系统开发的仿真模型涉及多个应用领域,具有多粒度、阶段相关性等的特性.本文提出了C4ISR系统开发的仿真模型体系,给出了仿真模型的规范化描述....     

高官能度水性聚氨酯丙烯酸酯/纳米SiO2杂化材料的制备及性能

以聚己内酯二醇(PCL)、异佛尔酮二异氰酸酯(IPDI)、二羟甲基丙酸(DMPA)和季戊四醇三丙烯酸酯(PETA)为原料,合成了高官能度水性聚氨酯丙烯酸酯WPUA。以WPUA为有机相,γ-甲基丙烯酰氧丙基三甲氧基硅烷(TMSPM)改性纳米SiO2为无机相,制备了水性光固化有机/无机纳米杂化体系。通过傅立叶变换红外光谱对合成产物进行了表征,并对杂化薄膜的表面形貌、热稳定性、光固化动力学及力学性能进行了分析。结果表明合成了预期产物,杂化体系中改性纳米SiO2分散均匀稳定;随着SiO2含量的增加,材料的热稳定性、力学性能均有明显提高;不同SiO2条件下体系均保持了较高的光固化速率和最终凝胶含量。     

多弧离子镀CrNx涂层的工艺与摩擦磨损性能

为了改善发动机活塞环的摩擦学性能和提高其使用寿命,采用多弧离子镀技术在活塞环表面制备了不同N2含量和弧电流的CrNx硬膜,采用X射线衍射技术、扫描电子显微镜、纳米硬度仪和发动机台架试验装置,分别测试了薄膜相结构、表面形貌、纳米硬度和抗高温摩擦磨损性能。研究结果表明：当N2质量分数为45%时,薄膜纳米硬度相对较高,CrNx薄膜中主要以CrN（220）相为主;随着弧电流的增加,薄膜的表面颗粒尺寸增加,当弧电流为60A时,薄膜纳米硬度相对较高。与Cr电镀层活塞环相比,CrNx涂层活塞环具有较强的抗高温粘着磨损性能。